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Synthesis and Characterization of New Copoly(amide-imide)s Based on 1,3- bis[4,4'-(trimellitimido)phenoxy]propane and Fumaric acid | ||
Journal of the Iranian Chemical Research | ||
مقاله 6، دوره 3، شماره 1، اسفند 2010، صفحه 41-47 اصل مقاله (310.02 K) | ||
نویسندگان | ||
Khalil Faghihi* ؛ Akram Feyzi؛ Reza Mohammadi Pour | ||
Department of Chemistry, Faculty of Science, Arak University, Arak, 38156, Iran | ||
چکیده | ||
In this article six new copoly(amide-imide)s (11a-c) were synthesized through the direct polycondensation reaction of 1,3-bis[4,4'-(trimellitimido) phenoxy] propane (6) with 3,3'- diamino diphenyl sulfone (7), 4,4'-diaminodiphenyl ether (8) and 1,5-naphtalene (9) in the presence of fumaric acid (10) as a second diacid in a medium consisting of N-methyl-2- pyrrolidone, triphenyl phosphite, calcium chloride and pyridine. The resulted polymers were fully characterized by means of FT-IR spectroscopy, elemental analyses, inherent viscosity, and solubility tests. Thermal stabilities of a polymer (11a-c) were investigated by using TGA & DTG thermograms. | ||
کلیدواژهها | ||
High performance polymers؛ Copoly(amide-imide)s؛ Direct polycondensation | ||
مراجع | ||
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