Microwave-assisted thioacetalization of carbonyl compounds using Al-MCM-41 as an efficient heterogeneous catalyst

Journal of Chemical Reactivity and Synthesis

مقاله 5، دوره 2، شماره 1، مرداد 2012، صفحه 22-27   

نوع مقاله: Research Article

نویسندگان

Marzieh Abedini¹؛ Soheil Sayyahi^{* 2}

¹Department of Chemistry, Omidieh Branch, Islamic Azad University, Omidieh, Iran

²Department of Chemistry, Mahshahr Branch, Islamic Azad University, Mahshahr, Iran

چکیده

In this project various types of carbonyl compounds were efficiently converted to their corresponding 1,3-oxathiolanes  with 2-mercaptoethanol in the presence of catalytic amount of Al-MCM-41 with microwave energy. The catalyst can be reused several times without loss of its catalytic activity. Very short reaction times, reusability of the catalyst, and easy workup are noteworthy advantages of this method.

کلیدواژه‌ها

Al-MCM-41؛ Heterogeneous catalyst؛ 1؛ 3-oxathiolanes؛ Carbonyl compound؛ microwave energy