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Rostami, Sedigheh, Azizi, Seyed Naser, Rigi, Fatemeh. (1396). Efficient synthesis of 2,3-dihydroquinazolin-4(1H)-ones using nano-sized protonated ZSM–5 as a biodegradable and reusable solid acid catalyst. نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 7(4), 267-276.
Sedigheh Rostami; Seyed Naser Azizi; Fatemeh Rigi. "Efficient synthesis of 2,3-dihydroquinazolin-4(1H)-ones using nano-sized protonated ZSM–5 as a biodegradable and reusable solid acid catalyst". نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 7, 4, 1396, 267-276.
Rostami, Sedigheh, Azizi, Seyed Naser, Rigi, Fatemeh. (1396). 'Efficient synthesis of 2,3-dihydroquinazolin-4(1H)-ones using nano-sized protonated ZSM–5 as a biodegradable and reusable solid acid catalyst', نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 7(4), pp. 267-276.
Rostami, Sedigheh, Azizi, Seyed Naser, Rigi, Fatemeh. Efficient synthesis of 2,3-dihydroquinazolin-4(1H)-ones using nano-sized protonated ZSM–5 as a biodegradable and reusable solid acid catalyst. نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 1396; 7(4): 267-276.

Efficient synthesis of 2,3-dihydroquinazolin-4(1H)-ones using nano-sized protonated ZSM–5 as a biodegradable and reusable solid acid catalyst

Iranian Journal of Catalysis
مقاله 3، دوره 7، شماره 4، اسفند 2017، صفحه 267-276    اصل مقاله (1.17 M)
نوع مقاله: Articles
نویسندگان
Sedigheh Rostami1، 2؛ Seyed Naser Azizi* 1، 2؛ Fatemeh Rigi3
1Analytical division, Faculty of Chemistry, University of Mazandaran, Postal code 47416-95447, Babolsar, Iran.
2Nano and Biotechnology Research Group. University of Mazandaran, Babolsar, Iran.
3Department of Chemistry, Faculty of Sciences, University of Sistan and Baluchestan, Zahedan. Iran.
چکیده
Nano-sized protonated ZSM–5 ( H-ZSM-5nanozeolite) was successfully synthesized by the hydrothermal method using the bagasse ash (BGA) as a new silica source. Cultivated BGA in the south of the Caspian Sea (Mazandaran province, Iran) was used for extracting silica powder. H-ZSM-5 was characterized by Fourier transform infrared (FT-IR), X-ray diffraction (XRD), scanning electronic microscopy (SEM) and Brunauer–Emmett–Teller (BET), Barrett-Joyner-Halenda (BJH) techniques. The catalytic activity of H-ZSM-5 nanozeolite was evaluated for the synthesis of 2,3-dihydroquinazolin-4(1H)-ones via one-pot three-component reaction of aromatic aldehydes, 2-aminobenzothiazole or 2-aminobenzimidazole and isatoic anhydride under solvent-free conditions. Short reaction time, high yields, a simple experimental procedure in the absence of any toxic solvents and recovery of catalyst are the advantages of this protocol.
کلیدواژه‌ها
H-ZSM-5 nanozeolite؛ 2,3-Dihydroquinazolin-4(1H)-ones؛ Hydrothermal؛ Bagasse؛ Catalyst
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