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Hashemi-Uderji, Somayeh, Abdollahi-Alibeik, Mohammad, Ranjbar-Karimi, Reza. (1397). Fe3O4@FSM-16-SO3H as a new magnetically recyclable nanostructured catalyst: synthesis, characterization and catalytic application for the synthesis of pyrano[2,3-c]pyrazoles. نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 8(4), 311-323.
Somayeh Hashemi-Uderji; Mohammad Abdollahi-Alibeik; Reza Ranjbar-Karimi. "Fe3O4@FSM-16-SO3H as a new magnetically recyclable nanostructured catalyst: synthesis, characterization and catalytic application for the synthesis of pyrano[2,3-c]pyrazoles". نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 8, 4, 1397, 311-323.
Hashemi-Uderji, Somayeh, Abdollahi-Alibeik, Mohammad, Ranjbar-Karimi, Reza. (1397). 'Fe3O4@FSM-16-SO3H as a new magnetically recyclable nanostructured catalyst: synthesis, characterization and catalytic application for the synthesis of pyrano[2,3-c]pyrazoles', نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 8(4), pp. 311-323.
Hashemi-Uderji, Somayeh, Abdollahi-Alibeik, Mohammad, Ranjbar-Karimi, Reza. Fe3O4@FSM-16-SO3H as a new magnetically recyclable nanostructured catalyst: synthesis, characterization and catalytic application for the synthesis of pyrano[2,3-c]pyrazoles. نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 1397; 8(4): 311-323.

Fe3O4@FSM-16-SO3H as a new magnetically recyclable nanostructured catalyst: synthesis, characterization and catalytic application for the synthesis of pyrano[2,3-c]pyrazoles

Iranian Journal of Catalysis
مقاله 9، دوره 8، شماره 4، اسفند 2018، صفحه 311-323    اصل مقاله (2.21 M)
نوع مقاله: Articles
نویسندگان
Somayeh Hashemi-Uderji1؛ Mohammad Abdollahi-Alibeik* 1؛ Reza Ranjbar-Karimi2
1Department of Chemistry, Yazd University, Yazd 89158-13149, Iran.
2Department of Chemistry, Faculty of Science, Vali-e-Asr University, Rafsanjan 77176, Iran.
چکیده
A three-component process for the one-pot synthesis of 6-amino-4-aryl-5-cyano-3-methyl-1-phenyl-1,4-dihydropyrano[2,3-c]pyrazoles is described by the three-component reaction of aldehydes, 3-methyl-1-phenyl-1H-pyrazol-5(4H)-one and malononitrile in the presence of Fe3O4@FSM-16-SO3H as an efficient magnetically recyclable mesoporous catalyst. Folded sheet mesoporous material (FSM-16) was prepared by intercalation of a layered, kanemite type sodium silicate with cetyltrimethylammonium (CTMA) ions in the presence of dispersed Fe3O4. The Fe3O4@FSM-16-SO3H was synthesized by sulfonation of Fe3O4@FSM-16 and characterized by FESEM, XRD, BET, VSM and FT-IR techniques. This protocol suggests benefits in terms of higher yields and short reaction time. In addition, the catalyst could be separated using an external magnet and is reusable many times without any significant loss of activity.
کلیدواژه‌ها
Magnetic nanoparticle؛ Fe3O4؛ FSM-16-SO3H, Folded sheet mesoporous silica؛ Pyranopyrazoles؛ Recoverable catalyst؛ Heterogeneous
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