Synthesis and characterizations of CoTiO3-clay nanocomposites by sol-gel method

International Journal of Nano Dimension

مقاله 5، دوره 1، شماره 2، اسفند 2010، صفحه 125-132   

نوع مقاله: Reasearch Paper

شناسه دیجیتال (DOI): 10.7508/ijnd.2010.02.005

نویسندگان

M. Enhessari^{* 1}؛ S. Nazari Moqhadam²؛ M. Kargar Razi³؛ S. Ghezelbashi²؛ M. Habibi Tootkani²

¹Department of Chemistry, Naragh Branch, Islamic Azad University, Naragh , Iran.

²Department of Chemistry, North Tehran Branch, Islamic Azad University, Tehran, Iran.

³Department of Chemistry, North Tehran Branch, Islamic Azad University, Tehran, Iran

چکیده

CoTiO3-clay nano-composites were synthesized via a conventional sol-gel method; the gel was calcinated at 500 - 800°C for 2 hours. The presence of rhombohedra phase of CoTiO3 in clay matrix was confirmed by XRD, FTIR, SEM. Cobalt titanate-clay nano-composites were prepared with 5-20%(w/w) by sol-gel method. The spectra results were investigated at 20% (w/w) concentration .The optimum condition for nano-composite preparation in 20 %( w/w) at 600°C is obtained.

کلیدواژه‌ها

CoTiO3 Clay؛ Nanocomposite؛ Sol-gel Method؛ X-ray diffraction؛ SEM؛ FT-IR