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Synthesis and Characterization of Fe3O4@APTES@MOF-199 Magnetic Nanocatalyst and Its Application in the Synthesis of Quinoxaline Derivatives | ||
| Iranian Journal of Catalysis | ||
| مقاله 6، دوره 11، شماره 1، خرداد 2021، صفحه 59-67 اصل مقاله (1.15 M) | ||
| نوع مقاله: Articles | ||
| نویسندگان | ||
| Sami Sajjadifar* ؛ Issa Amini؛ Mina Karimian | ||
| Department of Chemistry, Payame Noor University, PO BOX 19395-4697 Tehran, Iran | ||
| چکیده | ||
| In this research, design and synthesis of Fe3O4@APTES@MOF-199magnetic nanocatalyst nanoparticles as a novel, recyclable and heterogeneous catalyst was developed. The magnetic nanocatalyst was analyzed using various spectroscopic methods such as Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), powder X-ray diffraction (XRD), energy dispersive X‐ray (EDX), thermogravimetric analysis (TGA), vibrating sample magnetometer (VSM). The particle size of the nanocatalyst is about 15-96 nm. In addition, magnetic nanocatalysts have been successfully applied to the synthesis of quinoxaline derivatives with a range of derivatives. The crude compounds were isolated in 84-97% yields. The recyclability of the catalyst was evaluated up to 5 times, with no loss in catalysis activity. | ||
تازه های تحقیق | ||
● Fe3O4@APTES@MOF-199 magnetic nanocatalyst was used as a reusable magnetic nanocatalyst for the synthesis of quinoxalinederivatives. ● The catalyst was easily recovered and reused without any significant loss in catalytic activity. ● The method conforms to several of the guiding principles of green chemistry. ● This method has the ability to tolerate a good range of substitutions. ● This procedure has the shorter reaction times, high yield and agreement with the green chemistry protocols. | ||
| کلیدواژه‌ها | ||
| Metal-organic framework؛ Fe3O4@APTES@MOF-199؛ Quinoxaline؛ Nanocatalyst | ||
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| مراجع | ||
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