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Saleh Fekr, Somayeh, Ardjmand, Mehdi, Fazaeli, Reza, Rafizadeh, Mehdi. (1400). Preparation of Ag Loaded WO3 Nano Rod and Its Highly Efficient Degradation of Flumequine under Sunlight Irradiation. نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 9(1), 38-48. doi: 10.22034/jna.2021.1926352.1250
Somayeh Saleh Fekr; Mehdi Ardjmand; Reza Fazaeli; Mehdi Rafizadeh. "Preparation of Ag Loaded WO3 Nano Rod and Its Highly Efficient Degradation of Flumequine under Sunlight Irradiation". نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 9, 1, 1400, 38-48. doi: 10.22034/jna.2021.1926352.1250
Saleh Fekr, Somayeh, Ardjmand, Mehdi, Fazaeli, Reza, Rafizadeh, Mehdi. (1400). 'Preparation of Ag Loaded WO3 Nano Rod and Its Highly Efficient Degradation of Flumequine under Sunlight Irradiation', نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 9(1), pp. 38-48. doi: 10.22034/jna.2021.1926352.1250
Saleh Fekr, Somayeh, Ardjmand, Mehdi, Fazaeli, Reza, Rafizadeh, Mehdi. Preparation of Ag Loaded WO3 Nano Rod and Its Highly Efficient Degradation of Flumequine under Sunlight Irradiation. نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 1400; 9(1): 38-48. doi: 10.22034/jna.2021.1926352.1250

Preparation of Ag Loaded WO3 Nano Rod and Its Highly Efficient Degradation of Flumequine under Sunlight Irradiation

Journal of Nanoanalysis
دوره 9، شماره 1، فروردین 2022، صفحه 38-48    اصل مقاله (1.77 M)
نوع مقاله: Original Research Paper
شناسه دیجیتال (DOI): 10.22034/jna.2021.1926352.1250
نویسندگان
Somayeh Saleh Fekr1؛ Mehdi Ardjmand2؛ Reza Fazaeli* 3؛ Mehdi Rafizadeh4
1Department of Chemical engineering, Faculty of engineering, South Tehran Branch, Islamic Azad University, Tehran, Iran
2Chemical Engineering Department , South Tehran Branch ,Islamic Azad University, Tehran,Iran
3Department of Chemistry, Faculty of Engineering, South Tehran Branch, Islamic Azad University, Tehran, Iran
4Department of Polymer Engineering & Color Technology, Amirkabir University of Technology, P.O. Box 15875-4413, Tehran, Iran
چکیده
The aim of this study was to evaluate the efficiency of Ag/WO3 photocatalytic process for degradation of Flumequine (FL) antibiotic from aqueous solutions. In this study, WO3 and Ag/WO3 particles were synthesized and characterized using X-ray diffraction (XRD), Fourier-transform infrared spectroscopy (FTIR), scanning electron microscope (SEM), energy dispersive X-ray spectrometry (EDS)/Map, Brunauer, Emmett, Teller (BET)/Barrett, Joyner, Halenda (BJH) and UV–vis diffuse reflectance spectroscopy (DRS) techniques. The photocatalytic degradation of FL from aqueous solutions was studied by Ag/WO3 photocatalyst under sunlight irradiation. The response surface methodology (RSM) with Central Composite Design (CCD) with 4 variables was used to investigate the relationship between the obtained responses and process variables and optimize with Design Expert software. In this study, the effect of pH, time (min), photocatalyst mass (g) and FL concentration (mg/L) were evaluated at 5 levels. Finally, the software is the best point to achieve the highest degradation efficiency of FL 99.54%, in optimal conditions at pH 3.07, time 101.14 (min), photocatalyst mass 0.13 (g) and FL concentration 41.3 (mg/L).
کلیدواژه‌ها
Ag/WO3؛ photocatalyst؛ Degradation؛ response surface methodology
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