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Sid kalal, Hossein, Khanchi, Ali Reza, Konoz, Elahe, Khaki, Sara, Taghiof, Mohammad, Baghdadi, Majid, Ahmad Panahi, Homayon. (1391). Pre-concentration of ultra-trace furan in beverage samples and its determination by high performance liquid cromatography. نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 3(1), 113-118. doi: https://doi.org/10.1186/2228-5547-3-19
Hossein Sid kalal; Ali Reza Khanchi; Elahe Konoz; Sara Khaki; Mohammad Taghiof; Majid Baghdadi; Homayon Ahmad Panahi. "Pre-concentration of ultra-trace furan in beverage samples and its determination by high performance liquid cromatography". نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 3, 1, 1391, 113-118. doi: https://doi.org/10.1186/2228-5547-3-19
Sid kalal, Hossein, Khanchi, Ali Reza, Konoz, Elahe, Khaki, Sara, Taghiof, Mohammad, Baghdadi, Majid, Ahmad Panahi, Homayon. (1391). 'Pre-concentration of ultra-trace furan in beverage samples and its determination by high performance liquid cromatography', نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 3(1), pp. 113-118. doi: https://doi.org/10.1186/2228-5547-3-19
Sid kalal, Hossein, Khanchi, Ali Reza, Konoz, Elahe, Khaki, Sara, Taghiof, Mohammad, Baghdadi, Majid, Ahmad Panahi, Homayon. Pre-concentration of ultra-trace furan in beverage samples and its determination by high performance liquid cromatography. نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 1391; 3(1): 113-118. doi: https://doi.org/10.1186/2228-5547-3-19

Pre-concentration of ultra-trace furan in beverage samples and its determination by high performance liquid cromatography

International Journal of Industrial Chemistry
دوره 3، شماره 1، اسفند 2012، صفحه 113-118
نوع مقاله: research article
شناسه دیجیتال (DOI): https://doi.org/10.1186/2228-5547-3-19
نویسندگان
Hossein Sid kalal* 1؛ Ali Reza Khanchi1؛ Elahe Konoz2؛ Sara Khaki2؛ Mohammad Taghiof1؛ Majid Baghdadi3؛ Homayon Ahmad Panahi2
1NFCRS, Nuclear Science and Technology Research Institute, Atomic Energy Organization of Iran, P.O. Box 11365-3486, Kargar Shomali street, Tehran, Iran
2Department of Chemistry, Islamic Azad University, Central Tehran Branch, Tehran, Iran
3Graduate Faculty of Environment, University of Tehran, Tehran, Iran
چکیده
Background
Furan has been considered to be toxic and carcinogenic. In this research, a new method was applied for the pre-concentration of furan in beverage samples followed by high-performance liquid chromatography-ultraviolet detection (HPLC-UV) determination.
Results
Determination was carried out by a UV detection at 205 nm. Some of the most important parameters, including extraction solvent, extraction time, sample temperature and volume, helium flow rate and salt effect were investigated and optimized. Linear calibration curve was obtained over a concentration range of 0.005 to 0.3 μg/mL with coefficient of determination (R2 = 0.998). Limit of detection and relative standard deviation were obtained as 0.001 μg/mL and 2.21% (n = 5), respectively.
Conclusions
The proposed method was applied successfully for the determination of furan in beverage samples. Among them, cola had a detectable amount of furan.
کلیدواژه‌ها
Furan؛ Beverage samples؛ Pre-concentration؛ HPLC-UV
آمار
تعداد مشاهده مقاله: 26


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