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Tohidi, Seyed Hossein, Gholamzadeh, Sanaz, Ayatollah Zadeh Shirazi, Marziah, Novinrooz, Abdol Javad. (1393). Characterization of sol–gel derived CuO/SiO2 nanostructure on temperature. نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 5(3), 63-68. doi: https://doi.org/10.1007/s40090-014-0017-5
Seyed Hossein Tohidi; Sanaz Gholamzadeh; Marziah Ayatollah Zadeh Shirazi; Abdol Javad Novinrooz. "Characterization of sol–gel derived CuO/SiO2 nanostructure on temperature". نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 5, 3, 1393, 63-68. doi: https://doi.org/10.1007/s40090-014-0017-5
Tohidi, Seyed Hossein, Gholamzadeh, Sanaz, Ayatollah Zadeh Shirazi, Marziah, Novinrooz, Abdol Javad. (1393). 'Characterization of sol–gel derived CuO/SiO2 nanostructure on temperature', نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 5(3), pp. 63-68. doi: https://doi.org/10.1007/s40090-014-0017-5
Tohidi, Seyed Hossein, Gholamzadeh, Sanaz, Ayatollah Zadeh Shirazi, Marziah, Novinrooz, Abdol Javad. Characterization of sol–gel derived CuO/SiO2 nanostructure on temperature. نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 1393; 5(3): 63-68. doi: https://doi.org/10.1007/s40090-014-0017-5

Characterization of sol–gel derived CuO/SiO2 nanostructure on temperature

International Journal of Industrial Chemistry
دوره 5، شماره 3، اسفند 2014، صفحه 63-68
نوع مقاله: research article
شناسه دیجیتال (DOI): https://doi.org/10.1007/s40090-014-0017-5
نویسندگان
Seyed Hossein Tohidi* 1؛ Sanaz Gholamzadeh2؛ Marziah Ayatollah Zadeh Shirazi3؛ Abdol Javad Novinrooz1
1Material Research School, Nuclear Science and Technology Institute, P. O. Box: 31485- 498, Karaj, Iran
2Computer Engineering and Information Technology Department, Amirkabir University, Tehran, Iran
3Islamic Azad University, Lahigan Branching, Guillan, Iran
چکیده
Various concentrations of copper are embedded into silica matrix to xerogels form using copper source—Cu(NO3)2·3H2O. The xerogel samples are prepared by hydrolysis and condensation of tetraethyl orthosilicate (TEOS) with determination of new molar ratio of components by the sol–gel method. CuO/SiO2 nanocomposite is prepared with mixture of components with new molar ratio of H2O/TEOS to be 6.2. In this investigation, the necessary amount of trihydrated copper nitrate is added to the solution in such a manner that the concentration of the copper oxide in final solution reaches 1, 2 and 5 wt% (samples A, B and C, respectively). After ambient drying, the gel samples are heated from 60 to 1,000 °C at a slow heating rate (50 °C/h). Thermal treatment effect is characterized by Fourier transmission infrared, thermal gravimetric analysis, X-ray diffraction, transmission electron microscopy, scanning electron microscopy, surface analysis and thermal program reduction methods at different temperatures.
کلیدواژه‌ها
Copper oxide؛ Characterization؛ Nanocomposite؛ Thermal treatment
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تعداد مشاهده مقاله: 23


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