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Hasanudin, Hasanudin, Asri, Wan, Anindia, Jeniva, Suheryanto, Suheryanto, Fanani, Zainal, Rinaldi, Nino, Al Muttaqii, Muhammad. (1401). Diisopropyl Ether Production via Isopropanol Catalytic Dehydration over Zirconium Phosphate Modified Natural Zeolite. نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 12(4), 463-474. doi: 10.30495/ijc.2022.1965421.1961
Hasanudin Hasanudin; Wan Ryan Asri; Jeniva Rindi Anindia; Suheryanto Suheryanto; Zainal Fanani; Nino Rinaldi; Muhammad Al Muttaqii. "Diisopropyl Ether Production via Isopropanol Catalytic Dehydration over Zirconium Phosphate Modified Natural Zeolite". نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 12, 4, 1401, 463-474. doi: 10.30495/ijc.2022.1965421.1961
Hasanudin, Hasanudin, Asri, Wan, Anindia, Jeniva, Suheryanto, Suheryanto, Fanani, Zainal, Rinaldi, Nino, Al Muttaqii, Muhammad. (1401). 'Diisopropyl Ether Production via Isopropanol Catalytic Dehydration over Zirconium Phosphate Modified Natural Zeolite', نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 12(4), pp. 463-474. doi: 10.30495/ijc.2022.1965421.1961
Hasanudin, Hasanudin, Asri, Wan, Anindia, Jeniva, Suheryanto, Suheryanto, Fanani, Zainal, Rinaldi, Nino, Al Muttaqii, Muhammad. Diisopropyl Ether Production via Isopropanol Catalytic Dehydration over Zirconium Phosphate Modified Natural Zeolite. نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 1401; 12(4): 463-474. doi: 10.30495/ijc.2022.1965421.1961

Diisopropyl Ether Production via Isopropanol Catalytic Dehydration over Zirconium Phosphate Modified Natural Zeolite

Iranian Journal of Catalysis
دوره 12، شماره 4، اسفند 2022، صفحه 463-474    اصل مقاله (1.18 M)
نوع مقاله: Articles
شناسه دیجیتال (DOI): 10.30495/ijc.2022.1965421.1961
نویسندگان
Hasanudin Hasanudin* 1، 2؛ Wan Ryan Asri1، 2؛ Jeniva Rindi Anindia1، 2؛ Suheryanto Suheryanto1، 2؛ Zainal Fanani1، 2؛ Nino Rinaldi3؛ Muhammad Al Muttaqii3
1Department of Chemistry, Faculty of Mathematics and Natural Science, Universitas Sriwijaya, Indralaya 30662, Indonesia
2Biofuel Research Group, Faculty of Mathematics and Natural Science, Universitas Sriwijaya, Indralaya 30662, Indonesia
3Research Center for Chemistry, National Research and Innovation Agency(BRIN-Indonesia), Science and Technology Park B.J. Habibie, Serpong, South Tangerang 15314, Banten Indonesia
چکیده
In this work, diisopropyl ether (DIPE) was produced through catalytic dehydration of isopropanol over zirconium phosphate-modified phosphate modified natural zeolite. The catalyst was prepared via the wet impregnation method. They were tested at 150 ˚C for 3 hours under a reflux system. The effect of zeolite-Zr(H2PO4)4 metal loading and zeolite-Zr without phosphate incorporation on dehydration isopropanol was also assessed. The results showed the natural zeolite was successfully modified as confirmed by XRD, FTIR, SEM-EDX, N2 physisorption, and catalyst acidity by the gravimetric technique. The highest isopropanol conversion (66.73%) was accomplished by 8 mEq/g zeolite-Zr(H2PO4)4 followed by the DIPE yield and selectivity up to 35.81% and 47.8%, respectively. Further reusability investigation showed that zeolite-Zr(H2PO4)4 catalyst provided adequate reusability up to the fourth reused with relatively decreased catalytic activity towards isopropanol dehydration.

تازه های تحقیق
  • The natural zeolite was modified via the wet impregnation method.
  • The natural zeolite was successfully modified as confirmed by XRD, FTIR, SEM-EDX, N2 physisorption, and catalyst acidity measurements.
  • The zeolite-Zr(H2PO4)4 had higher catalytic activity than zeolite-Zr towards isopropanol dehydration
  • The zeolite-Zr(H2PO4)4 catalyst (8 mEq/g metal loading) exhibited the highest isopropanol conversion, DIPE yield and selectivity, respectively.
  • Zeolite-Zr(H2PO4)4 catalyst provided adequate reusability up to the fourth reused towards isopropanol dehydration.
کلیدواژه‌ها
isopropanol conversion؛ diisopropyl ether؛ zeolite؛ modification؛ zirconium phosphate
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