اخبار و اعلانات

 آمار

تعداد نشریات418
تعداد شماره‌ها10,005
تعداد مقالات83,621
تعداد مشاهده مقاله78,323,203
تعداد دریافت فایل اصل مقاله55,372,415
Moghimi, A., Shabanzadeh, M.. (1391). Extraction and Determination of Trace Copper (II) Using Octadecyl Silica Membrane Disks Modified 1-(2-Pyridyl Azo) 2-Naphtol(Pan) in Water Samples and Paraffin-Embedded Tissues from Liver Loggerhead Turtles Specimens by FAAS. نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 2(2), -. doi: 10.22034/jchr.2012.543990
A. Moghimi; M. Shabanzadeh. "Extraction and Determination of Trace Copper (II) Using Octadecyl Silica Membrane Disks Modified 1-(2-Pyridyl Azo) 2-Naphtol(Pan) in Water Samples and Paraffin-Embedded Tissues from Liver Loggerhead Turtles Specimens by FAAS". نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 2, 2, 1391, -. doi: 10.22034/jchr.2012.543990
Moghimi, A., Shabanzadeh, M.. (1391). 'Extraction and Determination of Trace Copper (II) Using Octadecyl Silica Membrane Disks Modified 1-(2-Pyridyl Azo) 2-Naphtol(Pan) in Water Samples and Paraffin-Embedded Tissues from Liver Loggerhead Turtles Specimens by FAAS', نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 2(2), pp. -. doi: 10.22034/jchr.2012.543990
Moghimi, A., Shabanzadeh, M.. Extraction and Determination of Trace Copper (II) Using Octadecyl Silica Membrane Disks Modified 1-(2-Pyridyl Azo) 2-Naphtol(Pan) in Water Samples and Paraffin-Embedded Tissues from Liver Loggerhead Turtles Specimens by FAAS. نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 1391; 2(2): -. doi: 10.22034/jchr.2012.543990

Extraction and Determination of Trace Copper (II) Using Octadecyl Silica Membrane Disks Modified 1-(2-Pyridyl Azo) 2-Naphtol(Pan) in Water Samples and Paraffin-Embedded Tissues from Liver Loggerhead Turtles Specimens by FAAS

Journal of Chemical Health Risks
مقاله 2، دوره 2، شماره 2، شهریور 2012    اصل مقاله (390.35 K)
شناسه دیجیتال (DOI): 10.22034/jchr.2012.543990
نویسندگان
A. Moghimi* 1؛ M. Shabanzadeh2
1Department of Chemistry, Varamin (Pishva) Branch , Islamic Azad University, Varamin, Iran
22Department of Chemistry, Damghan Branch, Islamic Azad University, Damghan, Iran
چکیده
A simple and reproducible method for the rapid extraction and determination of trace amounts of copper(II) ions using octadecyl-bonded silica membrane disks modified by 1-(2-Pyridyl Azo)2-Naphtol(PAN)and Atomic Absorption Spectrometry was presented. The method was based on complex formation on the surface of the ENVI-18 DISKTM disks followed by stripping of the retained species by minimum amounts of appropriate organic solvents. The elution was efficient and quantitative. The effect of potential interfering ions, pH, ligand amount, stripping solvent, and sample flow rate were also investigated. Under the optimal experimental conditions, the break-through volume was found to about 1000mL providing a preconcentration factor of 500. In the present study, we reported the application of preconcentration techniques still continues increasingly for trace metal determinations by flame atomic absorption spectrometry (FAAS) for quantification of Cu in Formalin-fixed paraffin-embedded (FFPE) tissues from Liver loggerhead turtles. The maximum capacity of the disks was found to be 389± 4 µg for Cu2+.The limit of detection of the proposed method was 5ng per 1000mL.The method was applied to the extraction and recovery of copper in different water samples.
کلیدواژه‌ها
Copper (II)؛ SPE؛ Octadecyl slica disks؛ AAS؛ 1-(2-Pyridyl Azo) 2-Naphtol (PAN) Formalin-fixed paraffin-embedded (FFPE)
مراجع
  1. H.J.M.Bowen.1979 .Enviromental Chemistery
  2. of the Elements, Academic Press, New York,
  3. -135 .
  4. L.E.Brand, W.G. Sunda,R.R.L. Guillard.1986
  5. J.Exp.Mar.Biol.Ecol.96:225.
  6. H.H. Taylor, J.M.Anstiss.1999, Mar. Freshwat.
  7. Res.50:907.
  8. F.M.M.Morel, R.J.M. Hudson, N.M.Price,
  9. Limnol.Oceanogr.36:1742.
  10. A.S.Gordan, 1992 Mar.Chem.38:1.
  11. J.W.Moffett, L.E.Brand, P.L. Croot,
  12. K.A.Barbeau1997 ,Limnol.Oceanoger. 42:789.
  13. P.L.Croot,J.W.Moffett, L.E.Brand,2000
  14. Limnol.Oceanogr.45:619.
  15. M.Wood, H.K.Wang, 1983
  16. Environ.Sci.Technol.17:582A.
  17. N.N.Greemwood, A.Eamshow, 1984
  18. Chemistery of Elements, Pergamon Press, New
  19. York.
  20. C.A.Burtis, E.R.Ashwood,Tiets 1999 Textbook
  21. of Clinical Chemistery, third ed.,
  22. Macmillan,New York.
  23. B. Wetz, 1985 Atomic Absorption
  24. Spectroscopy, VCH, Amsterdam.
  25. A.D.Eaton, L.S.Clesceri, A.E.Greenberg, 1995
  26. Standard Methods for the examination of water
  27. and waste water ,19 th ed ,American Public
  28. Health Association, Washington,DC .
  29. F.J.Welcher, E.Boschmann, 1979 Organic
  30. Reagents for Copper, Krieger Huntington, New
  31. York.
  32. Z.Marczenko, 1986 Separation and
  33. Spectrophotometric Determination of
  34. Elements,Ellis Horwood, London.
  35. O.P.Bharagava, 1969 Talanta 16:743.
  36. A.A. Schilt, W.C. Hoyle, 1964Anal. Chem.
  37. :344.
  38. L.G.Borchart, J.P. Butler, 1957 Anal. Chem.
  39. :414.
  40. R. Chaisuksant, W.P. Ayuthaya, K. Grudpan,
  41. Talanta 53:579.
  42. D. Kara, M. Alkan, 2002 Microchem. J. 71: 29.
  43. K.Saito, S.Murakami, A. Muromatsu,
  44. E.Sekido, 1994 Anal.Chim. Acta 294:329.
  45. K. Ikeda, S. Abe, 1998 Anl.Chim. Acta 363:
  47. S. Igarashi, N. Ide, Y.Takagai, 2000
  48. Anal.Chim. Acta 424:263.
  49. J. Liu, W.Wang, G. Li, 2001Talanta 53:1149.
  50. A.N.Anthemidis, G.A. Zachariadis, J.A. Stratis,
  51. Talanta 54:935.
  52. D. Zenedelovska, G. Pavlovska, K. Cundeva,
  53. T.Stafilov, 2001 Talanta 54:139.
  54. M.Endo, K.Suziki, S.Abe, 1998 Anal. Chim.
  55. Acta 364:13.
  56. M.E. Campderros, A. Acosta, J. Marchese,
  57. Talanta 47:19.
  58. I.Narin, M. Soylak, L.Elic, M.Dogan, 2000
  59. Talanta 52:1041.
  60. Y.Akama, M.Ito, S.Tanaka, 2000 Talanta
  61. :645.
  62. K.Ohta, H.Tanahasi, T. Suzuki, S.Kaneco,
  63. , Talanta 53:715.
  64. V.Cuculic, M.Mlakar, M.Branica, Anal. Chim.
  65. Acta 339:(1997)181.
  66. A.Moghimi, M.S.Tehrani, S.Waqif Husain,
  67. Material Science Research India 3(1a)
  68. :27.
  69. M.S.Tehrani, A.Moghimi, S.Waqif Husain,
  70. Material Science Research India 3(2)
  71. :135.
  72. E.M.Thurman,M.S.Mills, 1998 Solid-Phase
  73. Extraction, Principles and Practice, Wiley, New
  74. York.
  75. J.Pawliszyn, 1997 Solid-Phase Microextraction,
  76. Theory and Practice, Wiley-VCH, New York.,
  77. R.M. Izatt, J.S. Bradshaw, R.L. Bruening, 1996
  78. Pure Appl. Chem. 68:1237.
  79. D.F.Hagen, C.G.Markell, G.A. Schmitt, 1990
  80. Anal.Chim. Acta 236:157.
  81. C.J.Krueger, J.A. Fild, 1995 Anal.Chem.
  82. :3363.
  83. K.Z.Taylor, D.S.Waddell,E.J.Reiner, 1995
  84. Anal. Chem. 67:1186.
  85. Y.Yamini, M.Ashraf-Khorassani, 1994 J.High
  86. Resolut. Chromatogr.17:634.
  87. M.Shamsipur, A.R.Ghiasvand, Y.Yamini, 1999
  88. Anal.Chem. 71:4892.
  89. M.Shamsipur, A.R.Ghiasvand, H. Sharghi,
  90. Int. J.Environ. Anal.Chem. 82:23.
  91. Brunner, J.;Mokhir, A.;Kramer, R. 2003
  92. J.Am.Chem.Soc. 125:12410.
  93. Zelder, F.H.;Brunner, J.; Kramer, R. 2004
  94. Chem. Commun., 902.
  95. Boll, I.; Kramer, R.; Brunner, J.; Mokhir, A.
  96. J.Am.Chem. Soc. 27(2005)7849.
  97. Hagen, D.F.;Mrkell, C.G.; Schmitt, G.A.;
  98. Blevins, D.D.; Anal. Chim. Acta 236(1990)
  99. .
  100. Yamini, Y.; Alizadeh, N.; Shamsipur, M.; Anal.
  101. Chim. Acta 69(1997) 355.
  102. Petit de Pena, Y.; Gallego M.; Valcarcel, M.;
  103. Anal. Chem. 67:2524 .
  104. Alizadeh, N.; Naeimi, H.; Sharghi,H.;
  105. Samsipur,Polish, M.; 1999 Polish
  106. J.Chem.73:915.
  107. Moghimi A, Poursharifi M.J. 2011, Australian
  108. Journal of Basic and Applied Sciences, 5(6):
  109. -986 ,
  110. Choi,Y.S.;Choi,H.S. 2003 Bull.Korean Chem.
  111. Soc.24:222.
  112. Matoso,E.;Kubota,L.T.;Cadore,S. 2003
  113. STalanta 60:1105.
  114. Purachat, B.;
  115. Liawruangrath,S.;Sooksamiti,P.;Rattanaphani,S
  116. .;Buddhasukh, D.2001 Anal.Sci. 17:443.
  117. Ensafi,A.A.;Abbasi,S.;Rahimi
  118. Mansour,H.;Mohammad pour Baltork, I.
  119. Anal.Sci. 17:609.
  120. Saber Tehrani,M.; Rastegar,F.; Parchehbaf,
  121. A.;Rezvani,Z,2005.Chinese Journal of
  122. Chemistry 23:1437.
  123. Moghimi A, R. Ghiasi, 2008 J. Korean Chem.
  124. Soc., 52: 4.
  125. Moghimi A., 2007; Chinese Journal of
  126. Chemistry 12:1842-1847.
  127. Hashemi, O. R.; Kargar-Razi, M.; Raoufi, F.;
  128. Moghimi, A.; Aghabozorg, H.; Ganjali, M. R.
  129. Microchem. J. 69: 1
  130. Hashemi, O. R.; Raoufi, F.; Ganjali, M. R.;
  131. Moghimi, A.; Kargar-Razi, M.; Aghabozorg,
  132. H.; Shamsipur, M. 2000,Anal. Sci. 16: 1221.
  133. Ganjali,M R ; Pourjavid, M. R.; Hajiagha
  134. Babaei, L.;Niasari, M. S. 2004.Quim Nova 27:
  136. Ganjali,M. R.; Pourjavid, M. R.; Hajiagha
  137. Babaei, L.;Niasari, M. S. 2004.Ann. Chim.
  138. (Rome) 94: 47.
  139. Ganjali,M R.; Basiripour, F.; Niasari, M. S.
  140. Can. 2002 J. Anal. Sci. Spect. 47: 41
آمار
تعداد مشاهده مقاله: 3,580
تعداد دریافت فایل اصل مقاله: 856


سامانه مدیریت نشریات علمی. قدرت گرفته از سیناوب