Role of growth temperature in CVD synthesis of Carbon nanotubes from Ni-Co bimetallic catalysts

International Journal of Nano Dimension

مقاله 7، دوره 7، شماره 3، آبان 2016، صفحه 240-246   

نوع مقاله: Reasearch Paper

شناسه دیجیتال (DOI): 10.7508/ijnd.2016.03.007

نویسندگان

Sepideh Sadat Madani¹؛ Karim Zare^{* 1}؛ Mahmood Ghoranneviss²

¹Department of Chemistry, Science and Research Branch, Islamic Azad University, Tehran, Iran

²Department of Physics, Science and Research Branch, Islamic Azad University, Tehran, Iran

چکیده

The effect of temperature variation on the growth of Carbon Nanotubes (CNTs) using Thermal Chemical Vapor Deposition (TCVD) is presented. Nickel and Cobalt (Ni-Co) thin films on Silicon (Si) substrates were used as catalysts in TCVD technique. Acetylene gas was used in CNTs growth process at the controlled temperature ranges from 850-1000 ̊ C. Catalysts and CNTs characterization was carried out using Atomic Force Microscopy (AFM), Energy Dispersive X-ray (EDX), Field Emission Scanning Electron Microscopy (FESEM) and Raman spectroscopy. It was found that the CNTs diameters increased with the temperature. The CNTs diameters were continually increased from 70 nm to 180 nm in the temperature range. In addition, the degree of crystallinity of the grown CNTs decreased.

کلیدواژه‌ها

Carbon nanotubes؛ DC-sputtering؛ Ni-Co catalyst؛ TCVD؛ Temperature

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