Synthesis, characterization and using Fe3O4@SiO2@FeCl3 as a new nanocatalyst for aza-Michael reaction between amines and ethyl crotonate

Iranian Journal of Catalysis

مقاله 2، دوره 10، شماره 3، آذر 2020، صفحه 189-194   

نوع مقاله: Articles

نویسندگان

Hamid Parsa؛ Mohammad Javad Taghizadeh^* ؛ Mojtaba Mossavi؛ Jaber Hosseini

Department of Chemistry, Faculty of Science, Imam Hossein University, Tehran 16597, Iran.

چکیده

In this article, recyclable Fe₃O₄@SiO₂@FeCl₃ was synthesized and entirely characterized by various techniques including XRD, FT-IR, SEM, EDX and VSM analysis. The catalytic ability of produced Fe₃O₄@SiO₂@FeCl₃ was studied in the aza-Michael reaction of diethyl amine and ethyl crotonate which lead to high yield of product. Also, this procedure was used to synthesize other derivatives resulted from different amines. Synthesized Fe₃O₄@SiO₂@FeCl₃ nanocatalyst has some great advantages such as easy preparation method, simple recovery and high efficiency.

کلیدواژه‌ها

Aza-Michael reaction؛ Fe3O4@SiO2@FeCl3 nanocatalyst؛ α,β-Unsaturated carbonyl compounds

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مراجع

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