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Nikoofar, Kobra, Shahriyari, Fatemeh. (1399). n-Octyl-3-methylpipyridinium bromide ([OMePPy]+Br-): novel ionic liquid to promote green synthesis of polycyclic fused acridines. نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 10(4), 325-331.
Kobra Nikoofar; Fatemeh Shahriyari. "n-Octyl-3-methylpipyridinium bromide ([OMePPy]+Br-): novel ionic liquid to promote green synthesis of polycyclic fused acridines". نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 10, 4, 1399, 325-331.
Nikoofar, Kobra, Shahriyari, Fatemeh. (1399). 'n-Octyl-3-methylpipyridinium bromide ([OMePPy]+Br-): novel ionic liquid to promote green synthesis of polycyclic fused acridines', نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 10(4), pp. 325-331.
Nikoofar, Kobra, Shahriyari, Fatemeh. n-Octyl-3-methylpipyridinium bromide ([OMePPy]+Br-): novel ionic liquid to promote green synthesis of polycyclic fused acridines. نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 1399; 10(4): 325-331.

n-Octyl-3-methylpipyridinium bromide ([OMePPy]+Br-): novel ionic liquid to promote green synthesis of polycyclic fused acridines

Iranian Journal of Catalysis
مقاله 8، دوره 10، شماره 4، اسفند 2020، صفحه 325-331    اصل مقاله (937.07 K)
نوع مقاله: Articles
نویسندگان
Kobra Nikoofar* ؛ Fatemeh Shahriyari
Department of Chemistry, Faculty of Physics & Chemistry, Alzahra University, Tehran, Iran
چکیده
In this research, various polycyclic fused acridines were synthesized via the highly efficient and green one-step four-component reaction between isatins, dimedone, various amines, and dimethylacetylenedicarboxylates (DMAD/DEAD) in the presence of n-octyl-3-methylpipyridinium bromide ([OMePPy]+Br-) as a newly prepared ionic liquid, in absolute green situations at room temperature under solvent-free conditions. The ionic liquid characterized by 1H NMR, 13C NMR, GC-MASS, TGA/ DTG, EDX, and FESEM techniques. Utilizing an eco-friendly and simply synthesized ionic liquid, green and economic reaction media, and preparing a wide range of polycyclic fused acridines in good yields are some highlighted aspects of the reported protocol.

تازه های تحقیق
  • Synthesis of acridines in the presence of ([OMePPy]+Br-) as an ionic liquid, in absolute green situations at room temperature.
  • Synthesizing a novel ionic liquid, n-octyl-3-methylpipyridinium bromide ([OMePPy]+Br-), form available substrates via a simple procedure.  
  • The ionic liquid ([OMePPy]+Br-) characterized by 1H NMR, 13C NMR, GC-MASS, TGA/ DTG, EDX, and FESEM techniques.
  • Performing a benign MCR by utilizing an eco-friendly and simply synthesized IL, in green and economic reaction media.
کلیدواژه‌ها
Acridines؛ Ionic liquid؛ Isatin؛ Multi-component reaction (MCR)؛ Green chemistry
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مراجع
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تعداد مشاهده مقاله: 289
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