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Sharifi Sharifabad, Saeed, Mirjalili, Bi Bi Fatemeh, Bamoniri, Abdolhamid. (1401). Nano-SiO2/Taurine as a new natural based catalyst for synthesis of hexahydroquinolines derivative. نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 12(3), 365-372. doi: 10.30495/ijc.2022.1959104.1936
Saeed Sharifi Sharifabad; Bi Bi Fatemeh Mirjalili; Abdolhamid Bamoniri. "Nano-SiO2/Taurine as a new natural based catalyst for synthesis of hexahydroquinolines derivative". نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 12, 3, 1401, 365-372. doi: 10.30495/ijc.2022.1959104.1936
Sharifi Sharifabad, Saeed, Mirjalili, Bi Bi Fatemeh, Bamoniri, Abdolhamid. (1401). 'Nano-SiO2/Taurine as a new natural based catalyst for synthesis of hexahydroquinolines derivative', نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 12(3), pp. 365-372. doi: 10.30495/ijc.2022.1959104.1936
Sharifi Sharifabad, Saeed, Mirjalili, Bi Bi Fatemeh, Bamoniri, Abdolhamid. Nano-SiO2/Taurine as a new natural based catalyst for synthesis of hexahydroquinolines derivative. نشریه علمی پژوهشی دانشگاه آزاد اسلامی, 1401; 12(3): 365-372. doi: 10.30495/ijc.2022.1959104.1936

Nano-SiO2/Taurine as a new natural based catalyst for synthesis of hexahydroquinolines derivative

Iranian Journal of Catalysis
مقاله 8، دوره 12، شماره 3، آذر 2022، صفحه 365-372    اصل مقاله (1.02 M)
نوع مقاله: Articles
شناسه دیجیتال (DOI): 10.30495/ijc.2022.1959104.1936
نویسندگان
Saeed Sharifi Sharifabad1؛ Bi Bi Fatemeh Mirjalili* 1؛ Abdolhamid Bamoniri2
1Department of Chemistry, College of Science, Yazd University, Yazd, P.O. Box 89195-741, Iran
2Department of Organic Chemistry, Faculty of Chemistry, University of Kashan, Kashan, Iran
چکیده
In this research work, Nano-SiO2/Taurine was synthesized and characterized by FT-IR, energy dispersive X-ray analysis (EDX), scanning electron microscopy (SEM), X-ray diffraction patterns (XRD) ,Thermogravimetric analysis (TGA) and MAP analysis. Nano-SiO2/Taurine has considerable benefits such as simple preparation protocol, simple handling, high acidic property, reusability and high stability. Nano-SiO2/Taurine was used as a catalyst for the synthesis of hexahydroquinolines by the reaction of ethyl acetoacetate, dimedone and ammonium acetate with various aldehydes. These reactions were carried out under solvent-free conditions at 85 °C. The present protocol is simple, eco-friendly and efficient. The hexahydroquinolines were produced at high yields and short reaction times.

تازه های تحقیق
  • Nano-SiO2/Taurine was prepared via reaction between nano silicagel and taurine.
  • Nano-SiO2/Taurine was characterized by FT-IR, energy dispersive X-ray analysis (EDX), X-ray diffraction patterns (XRD), scanning electron microscopy (SEM), Thermogravimetric analysis (TGA) and MAP analysis.
  • Nano-SiO2/Taurine was applied for the synthesis of hexahydroquinoline derivatives by the condensation reaction between ethyl acetoacetate, dimedone, ammonium acetate and various aldehydes.
  • Nano-SiO2/Taurine has considerable benefits such as simple preparation protocol, simple handling, high acidic property, reusability and high stability.
کلیدواژه‌ها
Nano-SiO2/Taurine؛ hexahydroquinoline؛ dimedone؛ ethyl acetoacetate
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